Title:

NMR Studies in Hexaborides Diplomarbeit in experimenteller Festkörperphysik.

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ISBN: 3817116829   ISBN: 3817116829   ISBN: 3817116829   ISBN: 3817116829 
 
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General Setup

The heart of the hardware installation is a Pentium II based personal computer with 400MHz CPU clock rate and 128MB RAM, mounted on a ASUS P2B ATX mother board with 100MHz bus clock, 4 PCI slots, 3 ISA slots and an AGP port. We have chosen that board mainly because it is one of the few which still has a sufficient number of ISA slots; we need the ISA slots for the GPIB card, the pulse card and the scope card, which we took over from an old installation and which are still based on that ancient standard. The computer is connected to the local network and to the internet (there is no remote control enabled; the system can only be used as a client) with a 10/100MBit ethernet card. It is running under Windows 98, since the seller of the cards provided his drivers for Windows 95 and since the program SeveNMR runs under Windows 3.11 for workgroups.

Most of the devices of our spectrometer have a GPIB port. A unique address has been given to each of them:

device GPIB address
   
LTC-10 15
PTS 310 16
HP 3497A 9
Le Croy 4
They are all connected to and controlled by the National Instruments NI-488.2 GPIB card in the computer. None of them is modern enough to support the new GPIB standard language. For further reference please consult [#!pts!#,#!niGPIB!#] and the other manuals.

The phase is not controlled by GPIB since GPIB has quite a low data transfer rate. In order to control the amplitude of the PTS by the computer it has to be switched to remote mode. This can be done by turning the amplitude button down to the click. The option to connect the Le Croy oscilloscope to the computer is only used for high resolution fast fourier transforms, where we average over many pulses before we read it out.

A driver provided by the manufacturer helps with the data transfer between SeveNMR and the hardware. In our software environment it is called D16gpib. It is a copy of TPWGPIB, the 16 bit version of the driver obtainable from National Instruments.

For generating the pulses we used a MR3020 Pulse Programmer from s.m.i.s. . It works completely independent of the rest of the computer and is therefore not affected by jams on the data bus or in the CPU due to other applications. The price to pay for this independence is that one has to program the card as a little computer in a Forth language. Since Forth is quite messy to handle, the manufacturer provides the card with a compiler which makes a more comfortable PPL language available and translates it to Forth. But SeveNMR contains an extended compiler which is adapted to our situation, knows some more commands such as adjusting the phase or opening the amplifier gate automatically and allows a very primitive program structure. But we will come to the pulse program compiler soon. The data transfer to the card is done by the shared library MRCOMS.DLL provided by the factory. In order to install them properly we added the two entries [MRCOMS] and [SMISDEFS] to WIN.INI.

The MR3020 Pulse Programmer generates rectangular pulses on 16 possible channels with a maximum time resolution of 100ns, a shortest duration of 300ns and a maximum duration of 16000s. The pulse programmer is in principle nothing else than a device which enables us to switch single bits in the output on and off. A pulse program therefore basically consists in setting the corresponding bits in a word (1 word = 2 bytes), sending it to the output and waiting an appropriate delay. In addition to that the Forth language also contains some commands to handle conditions and loops. In our setup the channels, denoted by the bits representing them, are connected as follows:

channel functionality
   
1 send rf pulse
4 open spectrometer gate
6 trigger
8 open amplifier gate
9 PTS phase mask
10 PTS phase mask
11 PTS latch
With the PTS phase mask one can change the phase of the pulse relative to the phase of the 10MHz output on the backside of the device, which are used for mixing the signal in the NMR spectrometer. This enables us to make phase sensitive measurements.

We used an IMTEC PC SCOPE board T12840 for the data acquisition. Using a PC board for the data acquisition implies the advantage of being much faster than using an external scope. The IMTEC board has two 8-bit channels, a sampling rate of maximum 20MHz in the two-channel mode and it offers the choice between 9 analog input ranges between $\pm$128mV and $\pm$64V. The card is triggered by an external trigger line; the trigger should be high during one dwell time. The data transfer is again done by using a dynamically linked library which we downloaded from the manufacturer's page.


next up previous contents
Next: SeveNMR Up: Computer Installation Previous: Computer Installation
  
Effekte der Physik und ihre Anwendungen (Taschenbuch)
von Manfred von Ardenne,
Gerhard Musiol,
Siegfried Reball
Siehe auch:
Grundkurs Theoretische Physik 2. Analytische Mechanik: v. 2 (Springer-Lehrbuch)
von Wolfgang Nolting
Experimentalphysik, Bd. 3. Atome, Moleküle und Festkörper
von Wolfgang Demtröder
Grundkurs Theoretische Physik 1. Klassische Mechanik
von Wolfgang Nolting
Klassische Elektrodynamik
von John D. Jackson
 
    
     

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